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Transition Metal-Catalyzed Couplings in Process Chemistry - Javier Magano, Joshua R Dunetz (Wiley-VCH, 2013) pdf

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 							ISBN 978-3-527-33279-3
  
  Transition metal-catalyzed coupling reactions have a rich history that led
to the awarding of the 2010 Nobel Prize in Chemistry to Professors Suzuki, Heck, and Negishi for their pioneering
contributions to the field. The coming of age of this active area of research is showcased in this
  book through
case studies in which process chemists from the pharmaceutical industry share their personal experiences developing
their own transition metal-catalyzed couplings for the large-scale manufacture of active pharmaceutical ingredients.
  
  Authors from Pfizer, Merck, Boehringer-Ingelheim, Novartis, Amgen, GSK, AstraZeneca, and other companies
describe the evolution of robust coupling processes from inception through early and late development, including
commercial routes where applicable. This book covers a wide range of coupling transformations while capturing the
lessons learned from each process. Every case study details the optimization of at least one transition metal-catalyzed
coupling while elaborating on issues such as design of experiments, scalability and throughput, product purification,
process safety, and waste management. The important issue of metal removal and the different technologies available to
accomplish this goal are also addressed. Finally, a section covers novel technologies for cross-coupling with high
potential for future applications on a large scale, such as microwave and flow chemistry as well as green
cross-couplings performed in water.
  
  With Forewords by Stephen L. Buchwald, Massachusetts Institute of
Technology, Trevor Laird, Editor of Organic Process Research and Development and Neal G. Anderson, Anderson's Process
Solutions LLC. 						

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